A new method for the reaction of cross-coupling: preparation of 5,5'-bi(1,10-phenanthroline)


Ağırtaş M. S.

HETEROCYCLIC COMMUNICATIONS, cilt.23, ss.7-8, 2017 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 23 Konu: 1
  • Basım Tarihi: 2017
  • Doi Numarası: 10.1515/hc-2016-0225
  • Dergi Adı: HETEROCYCLIC COMMUNICATIONS
  • Sayfa Sayısı: ss.7-8

Özet

Synthesis and characterization of 5,5'-bi(1,10-phenanthroline) (3) are described. Compound 3 was obtained by treatment of 5-chloro-1,10-phenanthroline (1) with 4-hydroxy-phthalonitrile (2) in the presence of K (2) CO (3) as a base in DMF at room temperature for 25 h.