Quantitative analysis of 1-hyoscyamine in Hyoscyamus reticulatus L. by GC-MS


Kartal M., Kurucu S., Altun L., Ceyhan T., Sayar E., Cevheroglu S., ...Daha Fazla

TURKISH JOURNAL OF CHEMISTRY, cilt.27, ss.565-569, 2003 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 27 Konu: 5
  • Basım Tarihi: 2003
  • Dergi Adı: TURKISH JOURNAL OF CHEMISTRY
  • Sayfa Sayıları: ss.565-569

Özet

The hyoscyamine content of leaves and root samples of Hyoscyamus reticulatus L. from Bulamk, Mus in east Anatolia, Turkey, was determined by capillary GC-MIS to be 0.036 +/- 0.004% in the leaves and 0.056 +/- 0.011% in the roots as the predominant compound. Sopolamine was only detected in trace amounts. These findings are in accordance with reports on hyoscyamine content in Hyoscyamus species. The limit of detection was 3.125 mug/mL and the limit of quantification was 6.25 mug/ml, for hyoscyamine. This method has been shown to be linear and sensitive.